3-Methoxy-2-methylbenzoic acid
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Product Name :
3-Methoxy-2-methylbenzoic acid
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CAS No :
55289-06-0
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Project State :
Commercial
Application
General Description
Cost-effective and customizable 3-Methoxy-2-methylbenzoic acid 55289-06-0 factory
- Molecular Formula:C9H10O3
- Molecular Weight:166.177
- Melting Point:147.0 to 151.0 °C
- Boiling Point:297 °C at 760 mmHg
- PKA:3.83±0.10(Predicted)
- Flash Point:119.9 °C
- PSA：46.53000
- Density:1.168 g/cm3
- LogP:1.70180
55289-06-0 Relevant articles
Preparation method of 6-chloro-2-methoxytoluene and synthesis process of methoxyfenozide
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, (2021/08/14)
The invention relates to the field of in...
Synthesis process 2 - methyl -3 - methoxybenzoic acid
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Paragraph 0024; 0029; 0045-0046; 0052-0053; 0059; 0062, (2021/10/20)
The invention discloses a synthesis proc...
2-methyl-3-methoxybenzoic acid and preparation method thereof
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Paragraph 0034; 0036-0038; 0040-0043; 0044-0046; 0048-0050, (2020/05/01)
The invention belongs to the field of co...
2-methyl-3-methoxybenzoyl chloride synthesizing process
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Paragraph 0018; 0022; 0023; 0027; 0028, (2019/03/15)
The invention discloses a 2-methyl-3-met...
55289-06-0 Process route
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603-80-5
3-hydroxy 2-methylbenzoic acid
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77-78-1
dimethyl sulfate
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55289-06-0
3-methoxy-2-methylbenzoic acid
| Conditions | Yield |
|---|---|
|
3-hydroxy 2-methylbenzoic acid;
With
sodium hydroxide;
In
water;
at 40 ℃;
pH=5.5 - 10.5;
dimethyl sulfate;
With
sodium hydroxide;
In
water;
at 40 - 45 ℃;
for 4h;
pH=10.4 - 10.6;
With
sodium hydroxide; sulfuric acid;
more than 3 stages;
|
90.4% |
|
at 55 - 65 ℃;
|
53.4% |
|
With
alkaline solution;
anschliessend Hydrolyse;
|
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10533-44-5,14455-35-7,71815-55-9,104768-26-5
trisodium 1,3,5-naphthalenetrisulfonate
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77-78-1
dimethyl sulfate
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55289-06-0
3-methoxy-2-methylbenzoic acid
| Conditions | Yield |
|---|---|
|
trisodium 1,3,5-naphthalenetrisulfonate;
With
calcium hydroxide; sodium hydroxide;
In
water;
at 190 - 280 ℃;
for 15.5h;
under 22202.2 Torr;
dimethyl sulfate;
With
sodium hydroxide;
In
water;
at 40 - 90 ℃;
for 5h;
pH=10.4 - 11;
|
72.1% |
|
trisodium 1,3,5-naphthalenetrisulfonate;
With
sodium hydroxide;
In
water;
at 190 - 280 ℃;
for 6.5h;
under 13801.4 Torr;
dimethyl sulfate;
With
sodium hydroxide;
In
water;
at 40 - 90 ℃;
for 5h;
pH=10.4 - 11;
|
60% |
55289-06-0 Upstream products
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31804-36-1
1-bromo-3-methoxy-2-methylbenzene
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42981-93-1
3-methoxy-2-methylbenzoic acid methyl ester
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77533-17-6
3-methoxy-2-methylbenzonitrile
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603-80-5
3-hydroxy 2-methylbenzoic acid
55289-06-0 Downstream products
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24487-91-0
3-methoxy-2-methylbenzoyl chloride
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627883-78-7
3-methoxy-2-methyl-benzoic acid ethyl ester
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95330-29-3
3-methoxy-2,N-dimethylbanzamide
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857651-74-2
2-bromomethyl-3-methoxy-benzaldehyde