4-tert-Butylphenyl-acetonitrile
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Product Name :
4-tert-Butylphenyl-acetonitrile
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CAS No :
3288-99-1
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Project State :
Commercial
Application
General Description
Cost-effective and customizable 4-tert-Butylphenyl-acetonitrile 3288-99-1 for sale
- Molecular Formula:C12H15N
- Molecular Weight:173.258
- Vapor Pressure:0.00665mmHg at 25°C
- Refractive Index:1.505
- Boiling Point:270.9 °C at 760 mmHg
- Flash Point:120.4 °C
- PSA：23.79000
- Density:0.95 g/cm3
- LogP:3.05018
4-tert-Butylphenyl-acetonitrile(Cas 3288-99-1) Usage
InChI:InChI=1/C12H15N/c1-12(2,3)11-6-4-10(5-7-11)8-9-13/h4-7H,8H2,1-3H3
3288-99-1 Relevant articles
Synthesis method of acaricide cyflumetofen intermediate p-tert-butyl phenylacetonitrile
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Paragraph 0027-0031; 0042-0049, (2019/01/14)
The invention discloses a synthesis meth...
A method of preparing P-tert-butyl benzyl cyanide
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Paragraph 0010; 0030; 0031; 0032; 0033; 0034; 0035-0038, (2017/04/07)
The invention discloses a method for pre...
Formamides as Lewis Base Catalysts in SNReactions—Efficient Transformation of Alcohols into Chlorides, Amines, and Ethers
Huy, Peter H.,Motsch, Sebastian,Kappler, Sarah M.
, p. 10145 - 10149 (2016/08/16)
A simple formamide catalyst facilitates ...
METHOD OF CONVERTING ALCOHOL TO HALIDE
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, (2017/01/02)
The present invention relates to a metho...
3288-99-1 Process route
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3972-56-3
4-(tert-butyl)chlorobenzene
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105-56-6
ethyl 2-cyanoacetate
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3288-99-1
4-tert-butylbenzyl cyanide
| Conditions | Yield |
|---|---|
|
ethyl 2-cyanoacetate;
With
potassium tert-butylate;
In
tert-butyl alcohol;
at 98 ℃;
for 0.5h;
under 3420.23 Torr;
Inert atmosphere;
4-(tert-butyl)chlorobenzene;
In
dimethyl sulfoxide; tert-butyl alcohol;
at 112 ℃;
for 2.5h;
under 3800.26 Torr;
Inert atmosphere;
With
water;
In
dimethyl sulfoxide; tert-butyl alcohol;
at 142 ℃;
for 5h;
under 6080.41 Torr;
Temperature;
Pressure;
Inert atmosphere;
|
97.7% |
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3972-65-4
1-bromo-4-tert-butylbenzene
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105-34-0
methyl 2-cyanoacetate
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3288-99-1
4-tert-butylbenzyl cyanide
| Conditions | Yield |
|---|---|
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1-bromo-4-tert-butylbenzene; methyl 2-cyanoacetate;
With
sodium t-butanolate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 80 ℃;
for 0.333333h;
under 2280.15 Torr;
Inert atmosphere;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 95 ℃;
for 1h;
under 3040.2 Torr;
Inert atmosphere;
With
water;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 130 ℃;
for 4h;
under 4560.31 Torr;
Inert atmosphere;
|
96.1% |
3288-99-1 Upstream products
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143-33-9
sodium cyanide
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19692-45-6
4-tert-butylbenzyl chloride
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18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene
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151-50-8
potassium cyanide
3288-99-1 Downstream products
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101287-62-1
3-(4-tert-butyl-phenyl)-3-cyano-2-oxo-propionic acid ethyl ester
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157592-45-5
(4-tert-butylphenyl)(pyridin-2-yl)methanone
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208719-05-5
2-(4-tert-Butyl-phenyl)-acetimidic acid ethyl ester
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3549-23-3
methyl 2-(4-tert-butylphenyl)acetate